101 Granny Squares by Carol Alexander PDF

By Carol Alexander

ISBN-10: 1573671681

ISBN-13: 9781573671682

Welcome to the fantastic international of granny squares! those loved motifs were a precious a part of our crochet background for good over a century and so they proceed to grace our models and houses in numerous inventive new methods. they are super-easy, transportable and you'll cause them to out of virtually whatever.

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SCH 2 Ph C5H5N CH 2 Ph The mechanism shown in Chart 9 is supported by the formation of (XXXVI) in small yield by the interaction of (I) with ethyl phenylmercaptoacetate in the presence of pyridine. Thiophenol, which would + PhSCH 2 C0 2 Et C5H5N + PhSCHC0 2 Et CH—C0 2 Et O (XXXVI) + (PhSH) -> PhSSPh I SPh 40 B. D. TIL AK be eliminated in the reaction sequence, was detected as diphenyl disulfide, which was isolated and characterized. 67 Interaction of (I) with 2-mercaptomethylpyridine (A) in dimethyl formamide at room temperature proceeded as shown in Chart 10, giving 3,4-phthaloyl-2-thiaquinolizine (C) in low yield along with unreacted (I) and other products.

B. D. Tilak and R. V. Acharya, J. Sei. Ind. Bes. (India) 14B, 219 (1954). I. NAPHTHOQUINONOID DYES AND PIGMENTS 31 The mononaphthoquinonylamines are weakly substantive to cotton, although substantivity and fastness are improved by acylation of the free amino group with acid chlorides from benzoic, cinnamic, and azobenzene-4,4'-dicarboxylic acids to yield (LXXII). The bis naphthoquinonylamines (LXXIII) are, in general, more substantive to cotton and give fugitive violet shades. 54 2. 2,3-Phthaloylindoles 2-(o-Bromoarylamino)-3-chloro-l,4-naphthoquinones (LXXIV) when heated with copper powder in boiling nitrobenzene yield phthaloylindoles (LXXV).

Mathur, J. Sei. Ind. Res. (India) 17B, 33 (1958). 23 I. NAPHTHOQUINONOID DYES AND PIGMENTS I t is interesting to note t h a t whereas benzoylacetonitrile reacts with (I) in the presence of isoquinoline to yield (XLVII), the reaction when carried out in presence of pyridine does not yield a pyrrocoline derivative, but gives 2-phenyl-3-cyano[2,3-&]naphthofuran-4,9-dione (XLVIII). 3 3 2. Synthesis of 2,3-Phthaloylpyrrocolines by Ring Closure of Ylidene-enol Betaines Methylation of the pyridinium betainę (XX) with dimethyl sulfate yields 3-(2-methoxy-l ,4-naphthoquinonyl)pyridinium methosulfate (XLIX).

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101 Granny Squares by Carol Alexander


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